32601-86-8, 2-Chloro-3-methylquinoxaline is a quinoxaline compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated,32601-86-8
General procedure: Method A. To a solution of chloroheterocycles (2.5 mmol) inCHCl3 (25 mL) was added (0.69 g, 2.5 mmol) of N-cyclohexyldithiocarbamate cyclohexylammonium salt. The reaction mixture was refluxed at 61 C for 12 h. The reaction mixture wasevaporated under reduced pressure and 25 mL of ethanol wasadded to the solid residue. The yellowish-orange precipitatewas filtered to give the desired product. The crude compounds were pure enough for analytical purposes. Purification of products for analysis was achieved by crystallization from theappropriate solvent; chromatographed with the appropriateeluent or by repeated dissolution in KOH and reprecipitation byacetic acid. The filtrate was evaporated once again and the solidobtained was crystalized from ethanol water to give symmetrical dicyclohexylthiourea (3).
The synthetic route of 32601-86-8 has been constantly updated, and we look forward to future research findings.
Reference£º
Article; Fathalla, Walid; Ali, Ibrahim A. I.; Pazdera, Pavel; Beilstein Journal of Organic Chemistry; vol. 13; (2017); p. 174 – 181;,
Quinoxaline – Wikipedia
Quinoxaline | C8H6N2 | ChemSpider