212327-10-1, 7-Bromo-2-methoxyquinoxaline is a quinoxaline compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
[0211] To a solution of 7-bromo-2-methoxyquinoxaline (26.7 g, 0.11 mol, 1.0 eq.) in DMF (1100 mL) were added TEA (77.7 mL, 0.56 mol, 5.0 eq.), Et3SiH (71.2 mL, 0.45 mol, 4.0 eq.) and Pd(dppf)Cl2CH2Cl2 (4.56 g, 5.6 mmol, 0.05 eq.). The resulting mixture was stirred at 90 C in an autoclave for 12 h under CO (1 MPa), then cooled and concentrated. The resulting residue was purified via flash column chromatography (EA/PE=l/4, v/v) to afford 3-methoxyquinoxaline-6-carbaldehyde as a white solid (8.5 g, 40.5%yield).
212327-10-1, 212327-10-1 7-Bromo-2-methoxyquinoxaline 1237168, aquinoxaline compound, is more and more widely used in various fields.
Reference£º
Patent; NEUPHARMA, INC.; QIAN, Xiangping; ZHU, Yong-liang; WO2014/75077; (2014); A1;,
Quinoxaline – Wikipedia
Quinoxaline | C8H6N2 | ChemSpider