50998-17-9, 6-Bromoquinoxaline is a quinoxaline compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
50998-17-9, To a flask including 1 eq. of triphenylen-2-ylboronic acid and 1.2 eq. of 6-bromoquinoxaline, 0.03 eq. of Pd(dba)3, 0.06 eq. of (t-Bu)3P, and toluene (1 M) were added and refluxed with stirring for about 12 hours. Then, the reaction product was cooled to ambient temperature, extracted with methylene chloride and washed with distilled water. The product thus obtained was dried with MgSO4 and distilled under a reduced pressure, and the residue was separated by column chromatography to produce Compound B-1 (Yield 80.4%). The compound thus produced was identified using a high resolution mass spectrometer and 1H NMR. The mass of the synthesized compound thus identified was 355. [HRMS for C26H16N2 [M]+: calcd: 356.43, found: 355, Elemental Analysis for C26H16N2 calcd: C, 87.62; H, 4.52; N, 7.86].
50998-17-9 6-Bromoquinoxaline 610939, aquinoxaline compound, is more and more widely used in various fields.
Reference£º
Patent; SAMSUNG DISPLAY CO., LTD.; JEONG, Hyein; LEE, Jungsub; (58 pag.)US2017/162796; (2017); A1;,
Quinoxaline – Wikipedia
Quinoxaline | C8H6N2 | ChemSpider