6925-00-4, Quinoxaline-6-carboxylic acid is a quinoxaline compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated,6925-00-4
In a [11 3] neck flask was placed Quinoxaline-6-carboxylic acid (20.2 g) in 500 ml of THF. To this solution was slowly added [THIONYLCHLOLIDE] [(42ML,] [5EQ.).] The reaction mechanically stirred was warmed up to reflux and followed by HPLC quenching the sample with NH40H. After 3h at reflux no more starting material was present, the solvent was removed under reduced pressure and [SOC12] was chased with toluene 3 times. The solid was suspended in 100 ml EtOAc and filtered to obtain 23.47g of a beige solid. HPLC : 1. [114MIN. IHNMR] (DMSO-d6) [69.] 01-7.40 (m, [5H).]
The synthetic route of 6925-00-4 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; APPLIED RESEARCH SYSTEMS ARS HOLDING N.V.; WO2004/7491; (2004); A1;,
Quinoxaline – Wikipedia
Quinoxaline | C8H6N2 | ChemSpider