32601-86-8, 2-Chloro-3-methylquinoxaline is a quinoxaline compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
To a suspension of NaH (33.7 mg, 842 muetaiotaomicron) in DMF (3 ml) at 0 under an argon atmosphere was added (6-(pyrrolidin-l-yl)pyridin-2-yl)methanol (0.1 g, 561 muiotaetaomicron) and 2-chloro-3- methylquinoxaline (150 mg, 842 muiotaetaomicron). The mixture was stirred at 0 for 2.5 firs. At 0 water was given to the reaction mixture. The product was extracted with EtOAc, washed with water, dried over MgSC^, filtered and evaporated. The crude product was purified by column chromatography using a CH2Cl2/MeOH gradient as eluent, providing the title compound (0.15 g, 83%) as off-white solid. MS: M = 321.1 (M+H)+
32601-86-8, 32601-86-8 2-Chloro-3-methylquinoxaline 236276, aquinoxaline compound, is more and more widely used in various fields.
Reference£º
Patent; F. HOFFMANN-LA ROCHE AG; HOFFMANN-LA ROCHE INC.; FLOHR, Alexander; GROEBKE ZBINDEN, Katrin; KOERNER, Matthias; LERNER, Christian; WO2013/178569; (2013); A1;,
Quinoxaline – Wikipedia
Quinoxaline | C8H6N2 | ChemSpider