Mussinan, Cynthia J. et al. published their research in Journal of Agricultural and Food Chemistry in 1973 |CAS: 34413-35-9

The Article related to pyrazine compound cooked beef, flavor cone cooked beef, Foods: Animal Origin and other aspects.Safety of 5,6,7,8-Tetrahydroquinoxaline

Mussinan, Cynthia J.; Wilson, Richard A.; Katz, Ira published an article in 1973, the title of the article was Isolation and identification of pyrazines present in pressure-cooked beef.Safety of 5,6,7,8-Tetrahydroquinoxaline And the article contains the following content:

Flavor concentrations were isolated from beef cooked superatmospherically at 162.7.degree. by simultaneous steam distillation and continuous solvent extraction Separation and identification were accomplished by gas chromatog. and coupled gc-mass spectrometry. Mass spectral identifications were confirmed by IE values. A total of 33 pyrazines were identified. The experimental process involved the reaction of 5,6,7,8-Tetrahydroquinoxaline(cas: 34413-35-9).Safety of 5,6,7,8-Tetrahydroquinoxaline

The Article related to pyrazine compound cooked beef, flavor cone cooked beef, Foods: Animal Origin and other aspects.Safety of 5,6,7,8-Tetrahydroquinoxaline

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Kinlin, Thomas E. et al. published their research in Journal of Agricultural and Food Chemistry in 1972 |CAS: 34413-35-9

The Article related to filbert roasted volatiles, Foods: Animal Origin and other aspects.COA of Formula: C8H10N2

Kinlin, Thomas E.; Muralidhara, Ranya; Pittet, Alan O.; Sanderson, Anne; Walradt, John P. published an article in 1972, the title of the article was Volatile components of roasted filberts.COA of Formula: C8H10N2 And the article contains the following content:

Roasted filbert volatiles were isolated using the following techniques: steam distillation followed by solvent extraction; condensation of volatiles given off during steam distillation; and mol. distillation followed by fractionation using preparative gas chromatog. Extracts and fractions were analyzed using open tubular columns. 187 compounds are reported for the 1st time from roasted filbert volatiles including alkyl, alkenyl, oxygenated, and alicyclic pyrazines; pyrroles; pyridines; thiols, thiazoles, thiophenes, and sulfides; furans; phenols; acids; lactones; esters; terpenes; aromatic aldehydes, alkanals, 2-alkenals, and 2,4-alkadienals; aliphatic and olefinic alcohols and ketones; and aliphatic and aromatic hydrocarbons. The experimental process involved the reaction of 5,6,7,8-Tetrahydroquinoxaline(cas: 34413-35-9).COA of Formula: C8H10N2

The Article related to filbert roasted volatiles, Foods: Animal Origin and other aspects.COA of Formula: C8H10N2

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Akiyama, M. et al. published their research in Journal of Food Science in 2007 |CAS: 34413-35-9

The Article related to brewed arabica coffee volatile determination solid phase microextraction, Food and Feed Chemistry: Analysis and other aspects.Related Products of 34413-35-9

On September 30, 2007, Akiyama, M.; Murakami, K.; Ikeda, M.; Iwatsuki, K.; Wada, A.; Tokuno, K.; Onishi, M.; Iwabuchi, H. published an article.Related Products of 34413-35-9 The title of the article was Analysis of the headspace volatiles of freshly brewed arabica coffee using solid-phase microextraction. And the article contained the following:

Headspace volatiles of freshly brewed drip coffee were investigated by gas chromatog./mass spectrometry (GC/MS) and gas chromatog./olfactometry (GC/O, CharmAnal.) analyses. For this purpose, a solid-phase microextraction (SPME) sampling method for the headspace volatiles of freshly brewed drip coffee was developed. SPME fiber coated with divinylbenzene (DVB)/carboxen/polydimethylsiloxane (PDMS) was selected from 6 types, and sampling time was determined at 2 min. The headspace coffee volatiles stayed constant in proportion for the 1st 2 min to keep the freshness of the brewed coffee aroma. Using this sampling method, the headspace volatiles of freshly brewed drip coffee (Ethiopian arabica coffee, roast degree: L value; 23) were examined by GC/MS and GC/O analyses. From the GC/O results, 1-(3,4-dihydro-2H-pyrrol-2-yl)-ethanone (nutty-roast odor) and 4-(4′-hydroxyphenyl)-2-butanone (raspberry ketone, sweet-fruity odor) were newly detected as components in the aroma of coffee. The experimental process involved the reaction of 5,6,7,8-Tetrahydroquinoxaline(cas: 34413-35-9).Related Products of 34413-35-9

The Article related to brewed arabica coffee volatile determination solid phase microextraction, Food and Feed Chemistry: Analysis and other aspects.Related Products of 34413-35-9

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Baker, Richard R. et al. published their research in Food and Chemical Toxicology in 2004 |CAS: 34413-35-9

The Article related to tobacco smoke chem analysis flavoring additive, Toxicology: Methods (Including Analysis) and other aspects.Computed Properties of 34413-35-9

Baker, Richard R.; Pereira da Silva, Jose R.; Smith, Graham published an article in 2004, the title of the article was The effect of tobacco ingredients on smoke chemistry. Part I: Flavourings and additives.Computed Properties of 34413-35-9 And the article contains the following content:

The effects of 450 tobacco ingredients added to tobacco on the forty-four “Hoffmann analytes” in mainstream cigarette smoke have been determined These analytes are believed by regulatory authorities in the USA and Canada to be relevant to smoking-related diseases. They are based on lists published by D. Hoffmann and co-workers of the American Health Foundation in New York. The ingredients comprised 431 flavours, 1 flavor/solvent, 1 solvent, 7 preservatives, 5 binders, 2 humectants, 2 process aids and 1 filler. The cigarettes containing mixtures of the ingredients were smoked using the standard ISO smoking machine conditions. The levels of the “Hoffmann analytes” in the smoke from the test cigarettes containing the ingredient mixture were compared to those from control cigarettes without the ingredients. In practice, flavoring ingredients are typically added to tobacco that also contains casing ingredients and reconstituted tobacco materials. In order to keep the tobacco mixtures as authentic as possible, three comparisons have been made in this study. These are: (a) control cigarette containing a typical US blended, cased tobacco incorporating reconstituted tobacco vs. test cigarettes that had flavoring ingredients added to this tobacco; (b) control cigarette containing tobacco only vs. test cigarettes with the tobacco cased and incorporating flavorings; (c) control cigarette containing tobacco only vs. test cigarette incorporating additives made in an exptl. sheet material. The significances of differences between the test and control cigarettes were determined using both the variability of the data on the specific occasion of the measurement, and also taking into account the long-term variability of the anal. measurements over the one-year period in which analyses were determined in the present study. This long-term variability was determined by measuring the levels of the 44 “Hoffmann analytes” in a reference cigarette on many occasions over the one-year period of this study. The ingredients were added to the exptl. cigarettes at or above the maximum levels used com. by British American Tobacco. The effect of the ingredient mixtures on total particulate matter and carbon monoxide levels in smoke was not significantly different to the control in most cases, and was never more than 10% with any ingredient mixture It was found that, in most cases, the mixtures of flavoring ingredients (generally added in ppm levels) had no statistically significant effect on the analyte smoke yields relative to the control cigarette. Occasionally with some of the mixtures, both increases and decreases were observed for some smoke analyte levels relative to the control cigarette. These differences were generally up to about 15% with the mixtures containing flavoring ingredients. The significance of many of the differences was not present when the long-term variability of the anal. methodol. was taken into account. For the test cigarettes with ingredient mixtures containing casing ingredients, there were again no significant changes in smoke analyte levels in most cases. Those changes that were observed are as follows. Decreases in smoke levels were observed with some ingredient mixtures for most of the tobacco specific nitrosamines (up to 24%), NOx, most of the phenols (up to 34%), benzo[a]pyrene, and some of the aromatic amines and miscellaneous organic compounds on the “Hoffmann list”. Increases were observed for some test cigarettes in smoke ammonia, HCN, formaldehyde and lead levels (up to 24%). The significance of the ammonia and lead increases was not present when the long-term variability of the anal. methodol. was taken into account. The yields of some carbonyl compounds in smoke were increased in one comparison with an additives mixture containing cellulosic components; in particular, formaldehyde was increased by 68%. This was the largest single change seen in any smoke analyte level in this study. These carbonyls are produced from the pyrolysis of cellulosic and other polysaccharide materials, present in the additives mixture With this test cigarette, all tobacco specific nitrosamines, phenols, semi-volatile bases, NOx and some aromatic amines and miscellaneous organic compounds on the “Hoffmann list” were decreased, by up to 22%. The significance of many of these differences remained even when the long-term variability of the anal. methodol. was taken into account. The levels of all other “Hoffmann analytes” in the smoke were not significantly different to those of the control cigarette. With the exception of the determinations of “tar”, nicotine and carbon monoxide, there are currently no internationally recognized standard methods for measurement of the other “Hoffmann analytes”. Each laboratory uses its own methods and there are large laboratory-to-laboratory variations, as well as variations over time in a given laboratory Therefore, it is important that in any comparison of smoke analytes amongst different cigarettes, all the analytes should be measured in the same laboratory and at the same time. This was the case in the present study and all the methods have been validated internally. The experimental process involved the reaction of 5,6,7,8-Tetrahydroquinoxaline(cas: 34413-35-9).Computed Properties of 34413-35-9

The Article related to tobacco smoke chem analysis flavoring additive, Toxicology: Methods (Including Analysis) and other aspects.Computed Properties of 34413-35-9

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Lee, Changgook et al. published their research in Analytical Methods in 2015 |CAS: 34413-35-9

The Article related to volatile compound hsspme gcms ground coffee aroma, Food and Feed Chemistry: Beverages and other aspects.HPLC of Formula: 34413-35-9

Lee, Changgook; Lee, Younghoon; Lee, Jae-Gon; Buglass, Alan J. published an article in 2015, the title of the article was Improving the extraction of headspace volatile compounds: development of a headspace multi-temperature solid-phase micro-extraction-single shot-gas chromatography/mass spectrometry (mT-HSSPME-ss-GC/MS) method and application to characterization of ground coffee aroma.HPLC of Formula: 34413-35-9 And the article contains the following content:

A multi-temperature headspace solid-phase micro-extraction-single shot-gas chromatog./mass spectrometry (mT-HSSPME-ss-GC/MS) method has been developed for headspace anal. Three SPME fibers (50/30 μm DVB/CAR/PDMS) were used simultaneously for the extraction of volatile components from the headspace of a sample in three sample chambers at three different temperatures A cryo-focusing technique was adopted to avoid peak broadening and to maximize resolution during the sequential thermal desorption of the SPME fibers prior to a ‘single-shot’ chromatog. run. The method was developed and validated on a model ethanolic flavor mixture, containing 81 components. Comparison of mT-HSSPME-ss-GC/MS (10 min incubation time, then 30 min extraction time at 22, 50, and 70 °C extraction temperatures) with conventional SPME-GC/MS at a fixed temperature of 22, 50, or 70 °C showed that the former gave a headspace GC profile of the flavor mixture that was much closer to that of the syringe (direct) injection profile. None of the conventional headspace SPME extraction profiles were a good match to the syringe injection profile. The same technique applied to the headspace of coffee grounds gave a plentiful headspace volatile component profile compared to that of a single SPME anal. at a fixed single extraction temperature (22, 50, and 70 °C). The average percent recovery (defined for each component as 100 × mT-SPME (22 °C + 50 °C + 70 °C) TIC peak intensity divided by the arithmetic sum of individual temperature SPME (22 °C, 50 °C, 70 °C) TIC peak intensities) was 89.8% and 132 components were detected by mT-SPME-ss-GC/MS in the headspace of coffee grounds. The experimental process involved the reaction of 5,6,7,8-Tetrahydroquinoxaline(cas: 34413-35-9).HPLC of Formula: 34413-35-9

The Article related to volatile compound hsspme gcms ground coffee aroma, Food and Feed Chemistry: Beverages and other aspects.HPLC of Formula: 34413-35-9

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Zhou, Bin et al. published their research in Xiandai Shipin Keji in 2015 |CAS: 34413-35-9

The Article related to roasting volatile component coffee bean, Food and Feed Chemistry: Beverages and other aspects.Product Details of 34413-35-9

Zhou, Bin; Ren, Hong-tao published an article in 2015, the title of the article was Effect of roasting time on volatile components in Yunnan Arabica coffee.Product Details of 34413-35-9 And the article contains the following content:

Changes in the composition and content of volatile components in Yunnan Arabica coffee during roasting were studied. At a baking temperature of 230°C, the coffee was sampled at different baking times. Two anal. methods were used. Specifically, method one involved the simultaneous distillation and extraction of volatile components, and utilized gas chromatog.-mass spectrometry (GC-MS) to analyze volatile components in Yunnan Arabica coffee. Method two involved headspace direct sampling with GC-MS anal. The data in this study were analyzed quant. and qual., and by cluster anal. In the first method, a total of 160 kinds of volatile compounds were analyzed, and in the second method, 15 volatile compounds were analyzed. The data revealed that after baking for 6 min at 230°C, volatile components such as 2-Me pyrazine, furfuryl alc., 5-methyl-furan-aldehyde, and 2-ethy 1-5-methy 1-pyrazine were produced. Changes in the identity of the volatile components and their content in coffee were significant with increased baking time. According to the cluster anal., coffee roasting time could be divided into four categories, and it could be used as a way to identify degree of coffee roasting. The experimental process involved the reaction of 5,6,7,8-Tetrahydroquinoxaline(cas: 34413-35-9).Product Details of 34413-35-9

The Article related to roasting volatile component coffee bean, Food and Feed Chemistry: Beverages and other aspects.Product Details of 34413-35-9

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Ochiai, Nobuo et al. published their research in Journal of Chromatography A in 2013 |CAS: 34413-35-9

The Article related to silicone stir bar extraction odor compound tea water, eg silicone stir bar, gc–ms, multi-sbse ((m)sbse), odor analysis, pdms stir bar, thermal desorption, Food and Feed Chemistry: Analysis and other aspects.Product Details of 34413-35-9

On November 8, 2013, Ochiai, Nobuo; Sasamoto, Kikuo; Ieda, Teruyo; David, Frank; Sandra, Pat published an article.Product Details of 34413-35-9 The title of the article was Multi-stir bar sorptive extraction for analysis of odor compounds in aqueous samples. And the article contained the following:

As reproducible coating of stir bars with more polar phases was found to be very difficult, a supporting grid was used in the development of an ethyleneglycol-modified Silicone (EG Silicone) coated stir bar. This new polar coating showed good performance for the extraction of polar solutes, but long term use also showed degradation of the coating due to friction while stirring. In order to address the lower robustness of the EG Silicone stir bar which has a much softer coating compared to a conventional polydimethylsiloxane (PDMS) stir bar, a novel SBSE procedure termed multi-SBSE (mSBSE) was developed. mSBSE consists of the robust PDMS stir bar stirring at the bottom of the vial and the EG Silicone stir bar attached on the inner side wall of the vial (a magnetic clip is used for the set-up). After extraction, the two stir bars are placed in a single glass desorption liner and are simultaneously thermally desorbed. The desorbed compounds were analyzed by thermal desorption-gas chromatog.-mass spectrometry (TD-GC-MS). Compared to conventional SBSE, mSBSE provides more uniform enrichment of a wide range of odor compounds in aqueous sample since both stir bars can complement each other, while eliminating the damage of the EG Silicone phase during the extraction The robustness of the EG Silicone stir bar was dramatically increased and more than 30 extraction and desorption cycles were possible without loss in performance. The recoveries for polar solutes such as 2-acetyl pyrrole (log Kow: 0.55), benzyl alc. (log Kow: 1.08), guaiacol (log Kow: 1.34), and indole (log Kow: 2.05) were increased by a factor of about 2-7. The mSBSE-TD-GC-MS method showed good linearity (r2 > 0.9913) and high sensitivity (limit of detection: 0.011-0.071 ng mL-1) for the test compounds spiked in water. The feasibility and benefit of the method was demonstrated with anal. of odor compounds in roasted green tea. The normalized areas obtained from mSBSE showed the best enrichment for most of the selected compounds compared to conventional SBSE using the PDMS stir bar or the EG Silicone stir bar. Fifteen compounds were determined in the range of 0.15-210 ng mL-1 (RSD < 14%, n = 6). The experimental process involved the reaction of 5,6,7,8-Tetrahydroquinoxaline(cas: 34413-35-9).Product Details of 34413-35-9

The Article related to silicone stir bar extraction odor compound tea water, eg silicone stir bar, gc–ms, multi-sbse ((m)sbse), odor analysis, pdms stir bar, thermal desorption, Food and Feed Chemistry: Analysis and other aspects.Product Details of 34413-35-9

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Zhu, Meng-meng et al. published their research in Shipin Gongye Keji in 2014 |CAS: 34413-35-9

The Article related to qiaqia aroma sunflower seed volatility component gc ms analysis, Food and Feed Chemistry: Analysis and other aspects.Safety of 5,6,7,8-Tetrahydroquinoxaline

On March 15, 2014, Zhu, Meng-meng; Shen, Xu; Chen, Jiang-lin; Yang, Ting-ting; Hou, Ru-yan published an article.Safety of 5,6,7,8-Tetrahydroquinoxaline The title of the article was Analysis of the volatility components of Qiaqia aroma sunflower seeds and the research of formation mechanism. And the article contained the following:

The characteristic quality of the chem. composition of Qiaqia aroma sunflower seeds and the formation mechanism during the producing process were investigated, with the methods of simultaneous distillation and extraction (SDE) combining with GC-MS. This experiment made a comparison anal. of the volatility aroma components at the raw and Qiaqia aroma sunflower seeds which were boiled in solution of spices lots of times. From the kernel and in-shell of raw sunflower seeds it was identified in each 8 and 16 kinds of chem. composition Also, from the kernel and in-shell of aroma sunflower seeds, 88 and 91 kinds of chem. composition were identified, resp. The results showed that the aroma components and their contents which remained in the kernel and in-shell were different. Spice in boiling process remained in aroma sunflower seeds; it played an important role in the formation of flavor and quality of aroma sunflower seeds. And different spice component had different adsorption binding forces in different media of the in-shell and kernel. The results provided the tech. basis for further study of the formation mechanism under different producing processes. The experimental process involved the reaction of 5,6,7,8-Tetrahydroquinoxaline(cas: 34413-35-9).Safety of 5,6,7,8-Tetrahydroquinoxaline

The Article related to qiaqia aroma sunflower seed volatility component gc ms analysis, Food and Feed Chemistry: Analysis and other aspects.Safety of 5,6,7,8-Tetrahydroquinoxaline

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Lojzova, Lenka et al. published their research in Analytica Chimica Acta in 2009 |CAS: 34413-35-9

The Article related to pyrazine volatile aroma maillard reaction potato chip gc ms, Food and Feed Chemistry: Analysis and other aspects.Quality Control of 5,6,7,8-Tetrahydroquinoxaline

On May 8, 2009, Lojzova, Lenka; Riddellova, Katerina; Hajslova, Jana; Zrostlikova, Jitka; Schurek, Jakub; Cajka, Tomas published an article.Quality Control of 5,6,7,8-Tetrahydroquinoxaline The title of the article was Alternative GC-MS approaches in the analysis of substituted pyrazines and other volatile aromatic compounds formed during Maillard reaction in potato chips. And the article contained the following:

Several methods have been developed for the anal. of substituted pyrazines and related substances in potato chips. Following separation/detection approaches (all employing head-space solid phase microextraction, HS-SPME, for volatiles sampling), have been critically assessed in our study:. (i) gas chromatog.-ion trap mass spectrometry (GC-ITMS),. (ii) gas chromatog.-time-of-flight mass spectrometry (GC-TOFMS);. (iii) comprehensive two-dimensional gas chromatog.-time-of-flight mass spectrometry (GC × GC-TOFMS). Although in none of the tested systems full chromatog. resolution of some isomeric pairs could be achieved, the use of GC × GC-TOFMS offered the best solution, mainly because of distinctly lower limits of quantification (LOQs) for all of 13 target alkylpyrazines. In addition to good performance characteristics, a non-target screening and tentative identification of altogether 46 N-containing heterocyclic compounds (pyrazines, pyrrols, pyridines, pyrrolidinones, and tetrahydropyridines) was also enabled. The experimental process involved the reaction of 5,6,7,8-Tetrahydroquinoxaline(cas: 34413-35-9).Quality Control of 5,6,7,8-Tetrahydroquinoxaline

The Article related to pyrazine volatile aroma maillard reaction potato chip gc ms, Food and Feed Chemistry: Analysis and other aspects.Quality Control of 5,6,7,8-Tetrahydroquinoxaline

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Wu, Hua-chang et al. published their research in Zhongguo Tiaoweipin in 2012 |CAS: 34413-35-9

The Article related to yacai volatile flavor compound fermentation, hs spme gc ms, Food and Feed Chemistry: Analysis and other aspects.Category: quinoxaline

On October 10, 2012, Wu, Hua-chang; Zhang, Liang; Deng, Jing; Li, Ping-ping; Xiao, Chen; Shen, Fang published an article.Category: quinoxaline The title of the article was Annlysis of volatile flavor compounds in the process of Yacai fermentationed. And the article contained the following:

The headspace solid-phase microextraction coupled with capillary gas chromatog.-mass spectrometry(GC-MS) was used for the determination of volatile flavor compounds in Yacai with different fermentation times. A total of 75 volatile compounds were identified in these samples. And 29, 22, 21, 22, 22 and 27 kinds of volatile compounds were resp. identified from raw Yacai, new salted Yacai, salted 40 days Yacai, salted 80 days Yacai, salted 120 days Yacai and salted 160 days Yacai. Among these compounds, a series of compounds, such as acids, alcs., esters, and alkanes are the main volatiles contributing to flavor of Yacai. The experimental process involved the reaction of 5,6,7,8-Tetrahydroquinoxaline(cas: 34413-35-9).Category: quinoxaline

The Article related to yacai volatile flavor compound fermentation, hs spme gc ms, Food and Feed Chemistry: Analysis and other aspects.Category: quinoxaline

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